The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.

以异丙醇,醇内标,采用气相色谱-质谱法分析了卷烟烟气总粒相物中的游离乙酸,乙酸测定结果的相对标准差小于1%,平均回收率99。

The standard deviations were 0.06 and 0.14 for Phoxim and Quintozene repectively,while the coefficients of variation were 1.14% and 1.34%.The average recoveries were 99.5 and 99.2% separately.

辛硫磷五氯硝基苯标准差分别0.060.14,变异系数分别1.14%1.34%,平均回收率分别99.5%99.2%。